Full traceability and compliance glp, gmp, and fda 21 cfr. Then look no further than the aquacounter aq300 coulometric karl fischer titrator. Complete solutions for the volumetric and coulometric water content determination with karl fischer titration. The operating voltage is indicated on the specification plate. If you dont have adober reader r, click here to download the application. The measurement of samples which contain larger amounts of water require a lot of time and may exceed the capacity of. The end point of the titration is recorded using bivoltametric indication. Numerous substances cannot be analysed by direct karl fischer titration as they are not soluble, react with the karl fischer reagent or release their water only very slowly or not until heated to high temperatures. Barcode reader inmotion kf can out can connectionfor service use volumetric kf titrator 7. Spectralab volumetric karl fischer titrator has been designed for a wide range of water content application ranging from 10 ppm to 100% of moisture by volumetric method. Extensive automation and sample preparation options. This titrator was designed in germany as part of the hach titralab family of automatic titrators and allows you to quickly measure moisture content. Karl fischer moisture titrator di support model pdf data 4,774kb. Tests water in the range from 100 ppm to 100% simple and automatic titrant.
It can remote control the adp611 evaporator and visualize the evaporation curve on. Kem karl fischer coulometers can measure samples with a water content in the range of 10. Karl fischer titration is the method of choice for water content determination. The microprocessor with high performance controls automatically all electrolysis adjustments. Coulometric kf titrator manufacturer, exporter, supplier. At the end of the titration, the display will show the result in mg of h2o 5 ml of kf reagent. Safe handling of reagents, easier titration through automatic titration start. For optimal execution of the kf titration, the ph of the solution should be in the range between 4 and 8. With the new generation of mettler toledo compact volumetric and coulometric karl fischer titrators v20v30, c20c30 and excellence combined general and volumetric kf titrators t70 and t90, water determination has reached an unrivaled level of simplicity and security. Combining coulometry with the karl fischer method, aquamax kf titrators determine the water content of samples by measuring the amount of electrolysis current necessary to produce the required iodine this is an absolute technique which does not require the calibration of. Coulometric titrators are primarily used to analyse samples with a low water content. The optimum recording range is 10mg of water per sample.
The kf is an accurate, reliable and easy to use instrument for performing volumetric titrations in the laboratory. Each digital titrator comes with five delivery tubes and a methods manual, which covers the most commonly tested parameters and the corresponding titrant cartridges. Nonobservance of this provision may result in damage to the titroline. If an instrument is in continuous use, then more frequent testing intervals may be called for, e. Mettler toledo v20s compact volumetric kf titrators can analyze samples with water content between 100 ppm and 100% in single measurements or sample series with statistics. This procedure is applicable to calibrate the karl fischer apparatus, installed in the quality control department. Benchtop titrators mettler toledo easyplus easy ph titrators simplifies and speeds up automated acidbase endpoint or inflectionequivalence point titrations. Kf volumetric titrator for karl fischer titrations hach. Karl fischer moisture titrator coulometric titration kem kyoto. It is recommended that you repeat annually the testing of the instruments used for determining water content according to the karl fischer method. Using advanced control technology, this titrator gives the highest accuracy and precision in a minimum amount of time. Titrator or in personal injury or damage to property.
Karl fischer titration frequently asked questions metrohm. Kf titrator and immediately determine the water content of up to 14 samples. If you are looking for microprocessor kf moisture titrator, ma 101 c is truly high end instrument with many advantages since it is microcontroller based karl fischer titrator spectralab volumetric karl fischer titrator is automatic karl fischer titration apparatus designed for a wide range of water content ranging from 10 ppm to 100% of moisture by voltametric technique. With stateoftheart performance features, like a fritless cell option, the aq300 offers the same fast and accurate results youve come to expect from other. It consists of an electrolytic titration cell, dual platinum electrode, magnetic stirrer and control unit. New viewer program can show titration results recorded by kfwin. Karl fischer titrators clarkson laboratory and supply inc. Karl fischer moisture titrator volumetric titration. Pdf the volumetric karl fischer titration is concerned with the water. Hold the syringe at right angles directly in front of your eyes to read off the value. With it, water contents from a few ppm to 100% can be determined reliably and precisely in solid, liquid and gaseous samples.
The mkc710s titrator comes with a large tft colour touch screen. Find, read and cite all the research you need on researchgate. Karl fischer titrator ma 101c manufacturer, exporter. Hiranuma automated solid evaporator system aqs22010a the ev2010 automated evaporatorsample changer can be connected with both the aq2200a coulometric titrator and the aqv2200a volumetric titrator, which makes the aqs22010a a complete automated evaporation kf titration system. Pdf sample preparation in karl fischer titration researchgate. Integrating the titrator to a network is possible without further cost thanks to the integral ethernet connection. This viewer program can not only show all of titration results but also recalculate or simulate the data of these results. The coulometric karl fischer titrator titroline kf trace is the dedicated instrument for determining even smallest water content in your samples. Titrators we offer a variety of titrator products to meet your needs. Karl fischer titration is a method for moisture determination that is specific to water. Mettler toledo v20s compact volumetric kf titrator fisher. The new electrodes with definite identification are sending their specific data wireless to the titrator.
Pdf volumetric karl fischer titration researchgate. On a tight budget and looking for a reliable, easytouse coulometric karl fischer titrator. Operating instructions mettler toledo dl37 kf coulometer. The pocket titrator kf is a truly portable and easy to use coulometric titrator. Thank you for choosing a mettler toledo volumetric kf titrator.
Coulometric kf titrator mkc710s large user touch panel convenient operation. Volumetric karl fischer titration is suit able for samples with a water content in the range 100 ppm to 100 %. This method is a volumetric titration of water with karl fischer reagent which chemically reacts with water karl fischer reagent contains iodine, sulphurdioxide, pyridine and methanol quantitatively reacts. As opposed to other methods, such as drying ovens or infrared lamps, karl fischer titrators determine the actual water content in a sample, whereas other methods determine all volatile components that evaporate under the influence of heat. Voltametric kf titration back titration the automatic titrator is provided with twopoint auto calibration and standardization zero offset. The inexpensive 870 kf titrino plus is a kf titrator for volumetric water content determination. Product description aquamax kf plus titrators have been specifically designed for the determination of water content. Unpack the titrator karl fischer volumetric titrator.
It is also possible on any computer connected through lan to the main computer directly connected to the titrator by installing the viewer program. Kfwin software enables your pc to control kems kf moisture titrators including mkc710b, mkv710b, mkc520, mka520, mks520, mkc510n, mka510n and mks510n. With the dl37 you have the possibility to adapt the titration parameters control gain, end point indication, etc. Our titrator product offering includes electronic burettes, products for acidbase titrations, units with endpoint and equivalence point titration, meters for redox titrations, and products for karl fischer volumetric around 1% and coulometric at lower levels titrations. Determination of water content according to karl fischer direct method. The routine karl fischer titrator combines fast and precise water. Coulometric kf titrator c10sc20sc30s user manual 30297145c 7182017 10. Certain samples such as polymers require the use of kf oven in which the sample is heated and moisture in vapour form is taken to the titration vessel with a carrier gas. Karl fischer titrators for water moisture determination metrohm. Kfwin is designed to control the moisture titrator unit including start and reset of it, and set conditions and parameters of titration or sample materials from the pc. Highend volumetric and coulometric karl fischer titrators to determine any water content from 0.
Karl fischer moisture titrator coulometric titration mkc710m large color tftlcd with a touch panel 8. Suited for titralab kf series, automatic titrator model kf1121. Thanks to optional software control, these titrators afford you unmatched flexibility. Mettler toledo volumetric karl fischer titrator mettler toledo titrator family is developed by experts for a. The dual mode allows operation from the touchscreen or from the pc or from both. Coulometric kf titrator manufacturer, exporter, supplier coulometric titration process is a titration method in which constant current electrolysis is carried out using electrolytic control method. All results are stored in the labx database, independent of where it was started. Karl fischer determination is the benchmark for water content analysis. Karl fischer titration ruiz 2001 current protocols in. With its user interface, which is tailored to routine users, the 870 kf titrino plus is so simple to operate that only brief orientation periods are required. Automatic potentiometic and karl fischer volumetric titration. Karlfischer titration the method for determining water. With mettler toledo karl fischer titrators your operators need only to press.
Labx titration the software wizard for easy and secure titrations. The principle of the kf method was discovered by karl fischer, an engineer working for i. This video shows how to unpack the titrator and connect the power supply. With the mettler dl37 kf coulometer you can easily determine traces of water with a very high degree of accuracy. Ideal for fast and precise water content determination with easy operation. Print pdf page application pack for the determination of moisture content karl fischer. Repeat the same procedure by resetting the instrument to obtain 3 values for the factor of kf reagent which is not differing by 0. Omnis kf safe, easy, and fast karl fischer titration. Titrations with electrochemical reagent generation simple by one click in the userfriendly software. The instrument is capable of displaying ph and mv of the sample, with temperature compensation. Prior to switching the device on it has to be ensured that the operating voltage of titroline. Kf moisture titrator home page of kyoto electronics. The easy kfv titrates for water content in a wide variety of samples from any industry. Pdf this presentation is dedicated to a key issue in karl fischer titration, i.
To calibrate the equipment for reliable and accurate results. Using tightly sealed sample vials, the sample is inserted in the oven. The v20 is the ideal karl fischer volumetric titrator designed for a wide range of applications to determine water content in liquids and solids. Karl fischer titration is a classic titration method in chemical analysis that uses coulometric or. Applications of karl fischer titration newsmedical. Therefore the titroline 7000 uses always the correct calibration data. The mkc710s is ideally suited to measure samples which only release their water slowly or at elevated temperatures. Its straightforward operation and easy sample handling make stromboli an invaluable aid for many different industries such as pharmaceutical, polymer, petrochemical and specialty chemicals. The instrument has a grip for handheld operation or it can be clamped to a titrastir stir plate or laboratory stand for stationary setups. Karl fischer titrator, volumetric karl fischer titrators, ma.
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